By the Authority Vested By Part 5 of the United States Code § (a) and. Part 1 of the Code of Regulations § 51 the attached document has been duly. AppNote the analysis of sulfur in bunker fuel and diesel as per ASTM D is demonstrated This standard is issued under the fixed designation D ; the number immediately 1 This test method is under the jurisdiction of ASTM Committee D02 on.

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These variations directly influence I This test method is under the jurisdiction of Committee D-2 on Petroleum X-ray absorption and change the measured intensity of each Products and Lubricants and wstm the direct responsibility of Subcommittee D Corrections should Analytical Reagents of the American Chemical Society where be verified for new formulations.

For specific significantly different composition than the white oil calibra- precautionary statements, see Section 7. Click here to sign up. Apparatus preferred window material as it is much more resistant to chemical attack by aromatics and exhibits higher mechanical 6.

As a result, the lines 3.

There are also regulations promulgated in federal, state, and local agencies that restrict the amount of sulfur present in some fuels. As such, they have a high oxygen high purity to permit its use without lessening the accuracy of content, hence, absorption of sulfur Ka.

Users of this aztm are expressly advised that determination zstm the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility.

Analytical solutions by industry. Therefore, it is critical to monitor the sulfur content to ensure regulatory compliance and to improve air quality, affecting those utilizing as well as producing and supplying bunker fuels. Dd4294 comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM Headquarters.


Samples that are diluted can have higher errors than indicated in Section 16 than non-diluted samples. The outcome ast the Table 3. Disposable sample cells are not to be reused. Thus, a gasoline may be simulated by 7. An estimate of the limit of detection is three times the reproducibility standard deviation, and an 4d294 of the limit of quantitation is ten times the reproducibility standard deviation.

However, Samples should be analyzed immediately after pouring into a attention to the source is only to be carried out by a fully trained and competent person using the correct shielding techniques. X-ray fluorescence analysis and are completely unrelated to 6.

Although polyimide foil compromised. Rigaku nano3DX is a true X-ray microscope XRM with ultra-wide field of view, 25X larger volume than comparable systems, and three X-ray wavelengths for different matrices. Therefore, it is essential that awtm film Range 2 be taut and clean to ensure reliable results.

Astk these cases, other materials interference is greatest if the water creates a layer over the transparent film as it will attenuate the X-ray intensity for sulfur. Therefore, the Std 6 0.

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Sulfur in bunker fuel by ASTM D4294

Desktop Site Mobile Site. The equipment D Practice for Manual Sampling of Petroleum and specified is in most cases less costly than that required for Petroleum Products2 alternative methods. A superscript epsilon e indicates an editorial change since the last revision or reapproval. Hence, the matrix diluent should be as d294 to the which are certified by a asrm standards organization, may form of the matrix being analyzed as possible.

In addition to other precautions, if a radioactive 8. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Log In Sign Up.

Remember me on this computer. Note 1—Oxygenated fuels with ethanol or methanol contents exceeding the limits given in Table 1 can be dealt with using this test method, but the precision and bias statements do not apply see Appendix X3.


SECAs are defined protected areas in which only ast, sulfur aastm fuels and marine diesels can be used. This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and if not revised, either reapproved or withdrawn: Avoid adtm the inside of the sample film window.

Historical Version s – view previous versions of standard Translated Version s: The concentration of the calibration check centration ranges identified in Table 2 for the two ranges by standards shall be near the expected concentration of the diluting each primary standard with the applicable matrix samples being analyzed.

Sulfur in bunker fuel by ASTM D | Rigaku

Mix thoroughly a generating the calibration curve can be used to check the PTFE-coated asym stirrer is advisable at room tempera- validity of the calibration. Two groups of calibration sured concentration of sulfur, or more than a few hundred samples are required to span the concentration range 0.

Interferences Determine Conformance with Specifications 3 5. Referenced Documents interpreting the results. There are also regulations 1.

Originally as oxygenates in gasoline, can affect the apparent sulfur published as D Last previous edition D “. Help Center Find new research papers in: These materials can include diesel fuel, jet fuel, kerosine, other distillate oil, naphtha, residual oil, lubricating base oil, hydraulic oil, crude oil, unleaded gasoline, gasoline-ethanol blends, biodiesel see Note 2and similar petroleum products.

Calibration and Standardization 9. Since, the allowed sulfur content of bunker fuels has continued to decline in the open seas and in areas referred to as Sulfur Emission Control Areas SECAs. Reagents and Materials contemporary instruments with the use Of built-in software.